Solid-State DNP-NMR Spectrometer 263 GHz AVANCE™ III

Sensitivity Boost for Biomolecular NMR

The world’s first commercially available solid-state DNP-NMR spectrometer.

Bruker BioSpin’s 263 GHz AVANCE DNP-NMR Spectrometer is the world’s first commercially available solid-state DNP-NMR system. The 263 GHz spectrometer enables extended DNP solid-state NMR experiments delivering unsurpassed sensitivity for exciting new applications.

Signal enhancements from 20 to a factor of 80 on multiple samples are possible and system optimization is ongoing for even higher DNP efficiency. The new high power gyrotron system, delivering microwaves at 263 GHz, is robust, safe and easy-to-use, enabling long term DNP experiments without time limits.

Experiments performed at a low temperature of ~100 K benefit from the innovative low-temperature MAS probe that enables sample polarization in-situ, directly at the NMR field.

Main Features

Turn-key solution for DNP-enhanced solids NMR experiments at high field
Polarization enhancement yields factor up to 80 gain in sensitivity for solid-state NMR
Unique high power (25 W) 263 GHz microwave source
Easy to use software-controlled high power gyrotron (9.7 T)
Optimum beam propagation to the sample ensured by microwave transmission lines
New low-temperature MAS probe technology with built-in waveguide and cold spinning gas supply
AVANCE™ III 400 wide bore NMR system